Research of the Formation of Regularities Siloxane Norbornene Derivatives by Thermal Diels-Alder Reaction
| Parent link: | Procedia Chemistry Vol. 15 : Chemistry and Chemical Engineering in XXI century (CCE 2015).— 2015.— [P. 259-264] |
|---|---|
| Співавтори: | , |
| Інші автори: | , , , , |
| Резюме: | Title screen The methods of chromatography-mass spectrometry and 1H NMR-spectroscopy were used to study the reaction between dicyclopentadiene and vinyltriethoxysilane. The main reaction products are exo- and endo-isomers bicycle [2.2.1] hept-5-en-2-yl(triethoxy)silane. The overall yield of isomers is 55% of the load components. Co-products are the alkoxysilyl derivatives of dicyclopentadiene. Also the authors of the article paid attention to the problems of the time and temperature reaction, and ratios of starting components on chemical yield. Режим доступа: по договору с организацией-держателем ресурса |
| Опубліковано: |
2015
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| Предмети: | |
| Онлайн доступ: | http://dx.doi.org/10.1016/j.proche.2015.10.041 http://earchive.tpu.ru/handle/11683/15061 |
| Формат: | Електронний ресурс Частина з книги |
| KOHA link: | https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=645367 |
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| 200 | 1 | |a Research of the Formation of Regularities Siloxane Norbornene Derivatives by Thermal Diels-Alder Reaction |f V. G. Bondaletov [et al.] | |
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| 300 | |a Title screen | ||
| 320 | |a [References: р. 264 (6 tit.)] | ||
| 330 | |a The methods of chromatography-mass spectrometry and 1H NMR-spectroscopy were used to study the reaction between dicyclopentadiene and vinyltriethoxysilane. The main reaction products are exo- and endo-isomers bicycle [2.2.1] hept-5-en-2-yl(triethoxy)silane. The overall yield of isomers is 55% of the load components. Co-products are the alkoxysilyl derivatives of dicyclopentadiene. Also the authors of the article paid attention to the problems of the time and temperature reaction, and ratios of starting components on chemical yield. | ||
| 333 | |a Режим доступа: по договору с организацией-держателем ресурса | ||
| 461 | 0 | |0 (RuTPU)RU\TPU\network\3889 |t Procedia Chemistry | |
| 463 | 0 | |0 (RuTPU)RU\TPU\network\10324 |t Vol. 15 : Chemistry and Chemical Engineering in XXI century (CCE 2015) |o XVI International Scientific Conference dedicated to Professor L.P. Kulyov, 25-29 May 2015, Tomsk, Russia |f National Research Tomsk Polytechnic University (TPU) ; ed. E. I. Korotkova |v [P. 259-264] |d 2015 | |
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