Spark Plasma Sintering of Commercial Zirconium Carbide Powders: Densification Behavior and Mechanical Properties

Detalles Bibliográficos
Parent link:Materials
Vol. 8.— 2015.— [P. 6043-6061]
Autor Corporativo: Национальный исследовательский Томский политехнический университет (ТПУ) Институт неразрушающего контроля (ИНК) Кафедра физических методов и приборов контроля качества (ФМПК)
Otros Autores: Xialu Wei, Back C. Christina, Izhvanov O. Oleg, Grigorjev E. G. Evgeny Grigorjevich, Khasanov O. L. Oleg Leonidovich, Haines Ch. D. Christopher, Olevsky E. A. Evgeny Aleksandrovich
Sumario:Title screen
Commercial zirconium carbide (ZrC) powder is consolidated by Spark Plasma Sintering (SPS). Processing temperatures range from 1650 to 2100 °C. Specimens with various density levels are obtained when performing single-die SPS at different temperatures. Besides the single-die tooling setup, a double-die tooling setup is employed to largely increase the actual applied pressure to achieve higher densification in a shorter processing time. In order to describe the densification mechanism of ZrC powder under SPS conditions, a power-law creep constitutive equation is utilized, whose coefficients are determined by the inverse regression of the obtained experimental data. The densification of the selected ZrC powder is shown to be likely associated with grain boundary sliding and dislocation glide controlled creep. Transverse rupture strength and microhardness of sintered specimens are measured to be up to 380 MPa and 24 GPa, respectively. Mechanical properties are correlated with specimens’ average grain size and relative density to elucidate the co-factor dependencies.
Режим доступа: по договору с организацией-держателем ресурса
Lenguaje:inglés
Publicado: 2015
Colección:Manufacturing Processes and Systems
Materias:
Acceso en línea:http://dx.doi.org/10.3390/ma8095289
Formato: Electrónico Capítulo de libro
KOHA link:https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=644241

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200 1 |a Spark Plasma Sintering of Commercial Zirconium Carbide Powders: Densification Behavior and Mechanical Properties  |f Xialu Wei [et al.] 
203 |a Text  |c electronic 
225 1 |a Manufacturing Processes and Systems 
300 |a Title screen 
320 |a [References: p. 6058-6061 (52 tit.)] 
330 |a Commercial zirconium carbide (ZrC) powder is consolidated by Spark Plasma Sintering (SPS). Processing temperatures range from 1650 to 2100 °C. Specimens with various density levels are obtained when performing single-die SPS at different temperatures. Besides the single-die tooling setup, a double-die tooling setup is employed to largely increase the actual applied pressure to achieve higher densification in a shorter processing time. In order to describe the densification mechanism of ZrC powder under SPS conditions, a power-law creep constitutive equation is utilized, whose coefficients are determined by the inverse regression of the obtained experimental data. The densification of the selected ZrC powder is shown to be likely associated with grain boundary sliding and dislocation glide controlled creep. Transverse rupture strength and microhardness of sintered specimens are measured to be up to 380 MPa and 24 GPa, respectively. Mechanical properties are correlated with specimens’ average grain size and relative density to elucidate the co-factor dependencies. 
333 |a Режим доступа: по договору с организацией-держателем ресурса 
461 |t Materials 
463 |t Vol. 8  |v [P. 6043-6061]  |d 2015 
610 1 |a электронный ресурс 
610 1 |a труды учёных ТПУ 
610 1 |a карбид циркония (ZrC) 
610 1 |a искровое плазменное спекание 
610 1 |a степенные законы 
610 1 |a ползучесть 
610 1 |a прочность 
610 1 |a разрыв 
610 1 |a микротвердость 
701 0 |a Xialu Wei 
701 1 |a Back  |b C.  |g Christina 
701 1 |a Izhvanov  |b O.  |g Oleg 
701 1 |a Grigorjev  |b E. G.  |g Evgeny Grigorjevich 
701 1 |a Khasanov  |b O. L.  |c Russian physicist, materials scientist, Doctor of Engineering  |c professor, Director of TPU Nano-Centre and Head of the Department "Nanomaterials and Nanotechnologies" of TPU  |f 1958-  |g Oleg Leonidovich  |3 (RuTPU)RU\TPU\pers\27102  |9 12652 
701 1 |a Haines  |b Ch. D.  |g Christopher 
701 1 |a Olevsky  |b E. A.  |g Evgeny Aleksandrovich 
712 0 2 |a Национальный исследовательский Томский политехнический университет (ТПУ)  |b Институт неразрушающего контроля (ИНК)  |b Кафедра физических методов и приборов контроля качества (ФМПК)  |3 (RuTPU)RU\TPU\col\18709 
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856 4 |u http://dx.doi.org/10.3390/ma8095289 
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