Use of a Spline Function of a Fractional Degree for the Description of the Base Line in the Determination of Platinum by Stripping Voltammetry; Journal of Analytical Chemistry; Vol. 56, iss. 1

Dades bibliogràfiques
Parent link:Journal of Analytical Chemistry: Scientific Journal
Vol. 56, iss. 1.— 2001.— [P. 51-55]
Autor principal: Romanenko S. V. Sergey Vladimirovich
Autor corporatiu: Национальный исследовательский Томский политехнический университет (ТПУ)
Altres autors: Romanenko E. S. Eleanora Sergeevna, Kolpakova N. A. Nina Alexandrovna
Sumari:The systematic error in measuring the analytical signal of Pt obtained at a mercury thin-film electrode with staircase potential sweep has been studied. The description of the residual current by splines of degree 2.5 reduces the average systematic error by the factor of 4.3 as compared to the linear description. It is shown that splines of degree 2.5 are more stable as compared to the cubic splines, which suggests that the random error arising from the subtraction of the residual current is reduced when the spline degree decreases from 3 to 2.5.
Режим доступа: по договору с организацией-держателем ресурса
Idioma:anglès
Publicat: 2001
Matèries:
Accés en línia:http://dx.doi.org/10.1023/A:1026719512595
Format: MixedMaterials Electrònic Capítol de llibre
KOHA link:https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=642617

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200 1 |a Use of a Spline Function of a Fractional Degree for the Description of the Base Line in the Determination of Platinum by Stripping Voltammetry  |f S. V. Romanenko, E. S. Romanenko, N. A. Kolpakova 
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320 |a [References: p. 55 (11 tit.)] 
330 |a The systematic error in measuring the analytical signal of Pt obtained at a mercury thin-film electrode with staircase potential sweep has been studied. The description of the residual current by splines of degree 2.5 reduces the average systematic error by the factor of 4.3 as compared to the linear description. It is shown that splines of degree 2.5 are more stable as compared to the cubic splines, which suggests that the random error arising from the subtraction of the residual current is reduced when the spline degree decreases from 3 to 2.5. 
333 |a Режим доступа: по договору с организацией-держателем ресурса 
461 |t Journal of Analytical Chemistry  |o Scientific Journal 
463 |t Vol. 56, iss. 1  |v [P. 51-55]  |d 2001 
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