Influence of mechanical activation of initial reagents on synthesis of lithium ferrite; Russian Physics Journal; Vol. 55, iss. 6

التفاصيل البيبلوغرافية
Parent link:Russian Physics Journal: Scientific Journal
Vol. 55, iss. 6.— 2012.— [P. 672-677]
مؤلف مشترك: Национальный исследовательский Томский политехнический университет (ТПУ) Институт неразрушающего контроля (ИНК) Проблемная научно-исследовательская лаборатория электроники, диэлектриков и полупроводников (ПНИЛ ЭДиП)
مؤلفون آخرون: Surzhikov A. P. Anatoly Petrovich, Lysenko E. N. Elena Nikolaevna, Malyshev A. V. Andrei Vladimirovich, Pritulov A. M., Kazakovskaya O. G.
الملخص:Title screen
The influence of mechanical activation of the Li2CO3–Fe2O3 initial reagents on ferrite phase formation in lithium ferrite LiFe5O8 is investigated. Methods of x-ray powder diffraction (XRD) and thermomagnetometry with differential scanning calorimetry (TG(M)/DSC) are used to compare the efficiency of nonisothermal synthesis at identical temperatures and burning times of the initial and mechanically activated reagent mixtures. It is demonstrated that preliminary mechanical activation of the initial Li2CO3–Fe2O3 reagent mixture considerably increases the reactivity of the solid phase system, thereby allowing the temperature of the thermal synthesis of lithium ferrite LiFe5O8 to be decreased significantly.
Режим доступа: по договору с организацией-держателем ресурса
اللغة:الإنجليزية
منشور في: 2012
الموضوعات:
الوصول للمادة أونلاين:http://dx.doi.org/10.1007/s11182-012-9865-7
التنسيق: الكتروني فصل الكتاب
KOHA link:https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=639818
الوصف
الملخص:Title screen
The influence of mechanical activation of the Li2CO3–Fe2O3 initial reagents on ferrite phase formation in lithium ferrite LiFe5O8 is investigated. Methods of x-ray powder diffraction (XRD) and thermomagnetometry with differential scanning calorimetry (TG(M)/DSC) are used to compare the efficiency of nonisothermal synthesis at identical temperatures and burning times of the initial and mechanically activated reagent mixtures. It is demonstrated that preliminary mechanical activation of the initial Li2CO3–Fe2O3 reagent mixture considerably increases the reactivity of the solid phase system, thereby allowing the temperature of the thermal synthesis of lithium ferrite LiFe5O8 to be decreased significantly.
Режим доступа: по договору с организацией-держателем ресурса
DOI:10.1007/s11182-012-9865-7