Synthesis and X-ray crystal structure of the first dinuclear 1,1,2-tris(pyrazol-1-yl)ethene–zinc chloride complex

Bibliografiske detaljer
Parent link:Polyhedron: Scientific Journal
Vol. 33, iss. 1.— 2012.— [P. 252-256]
Andre forfattere: Potapov A. S. Andrey Sergeevich, Nudnova E. A., Ogorodnikov V. D., Petrenko T. V., Khlebnikov A. I. Andrey Ivanovich
Summary:Title screen
Complexes of 1,1,2-tris(pyrazol-1-yl)ethene (Pz3) with zinc(II), cadmium and mercury(II) ions were prepared and characterized by IR spectroscopy. Cadmium and mercury(II) complexes are insoluble solids of polymeric structure, while zinc complex is a discrete dinuclear complex (Pz3)2Zn2Cl4, the structure of which was determined by X-ray crystallography. Zinc complex contains five- and four-coordinated PzN4Cl and PzNCl3 zinc centers. Two Pz3 ligands in the complex are unequivalent, one of them is coordinated by two zinc centers in a bridging mode, while the other is a terminal ligand linked to only one of zinc ions.
Режим доступа: по договору с организацией-держателем ресурса
Sprog:engelsk
Udgivet: 2012
Fag:
Online adgang:http://dx.doi.org/10.1016/j.poly.2011.11.035
Format: Electronisk Book Chapter
KOHA link:https://koha.lib.tpu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=639664

MARC

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200 1 |a Synthesis and X-ray crystal structure of the first dinuclear 1,1,2-tris(pyrazol-1-yl)ethene–zinc chloride complex  |f A. S. Potapov [et al.] 
203 |a Text  |c electronic 
300 |a Title screen 
320 |a [References: p. 256 (32 tit.)] 
330 |a Complexes of 1,1,2-tris(pyrazol-1-yl)ethene (Pz3) with zinc(II), cadmium and mercury(II) ions were prepared and characterized by IR spectroscopy. Cadmium and mercury(II) complexes are insoluble solids of polymeric structure, while zinc complex is a discrete dinuclear complex (Pz3)2Zn2Cl4, the structure of which was determined by X-ray crystallography. Zinc complex contains five- and four-coordinated PzN4Cl and PzNCl3 zinc centers. Two Pz3 ligands in the complex are unequivalent, one of them is coordinated by two zinc centers in a bridging mode, while the other is a terminal ligand linked to only one of zinc ions. 
333 |a Режим доступа: по договору с организацией-держателем ресурса 
461 |t Polyhedron  |o Scientific Journal 
463 |t Vol. 33, iss. 1  |v [P. 252-256]  |d 2012 
610 1 |a электронный ресурс 
610 1 |a труды учёных ТПУ 
701 1 |a Potapov  |b A. S.  |c Chemist  |c Professor of Tomsk Polytechnic University, Doctor of chemical sciences  |f 1981-  |g Andrey Sergeevich  |3 (RuTPU)RU\TPU\pers\33909  |9 17482 
701 1 |a Nudnova  |b E. A. 
701 1 |a Ogorodnikov  |b V. D. 
701 1 |a Petrenko  |b T. V. 
701 1 |a Khlebnikov  |b A. I.  |c Chemist  |c Professor of Tomsk Polytechnic University  |f 1963-  |g Andrey Ivanovich  |3 (RuTPU)RU\TPU\pers\33927  |9 17500 
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